دانلود هندبوک میکرو استخراج با فاز جامد SPME نوشته Pawliszyn ویرایش 1

دانلود هندبوک میکرو استخراج با فاز جامد SPME نوشته Pawliszyn ویرایش 1

هندبوک تخصصی میکرو استخراج با فاز جامد SPME نوشته و تالیف پروفسور Pawliszyn که اولین بار این روش توسط ایشان بیان شده است از بهترین کتاب های تخصصی در زمینه آماده سازی نمونه و SPME می باشد.

در کتاب میکرو استخراج با فاز جامد به مباحثی همچون مدل سازی و انواع معادلات ریاضی ، روش های آماده سازی نمونه و تئوری SPME پرداخته شده است.

مشخصات کتاب 

• عنوان کتاب: Handbook of Solid Phase Microextraction
• فرمت فایل: PDF با کیفیت بالا و رنگی
• حجم فایل فشرده: 7.77 مگابایت
• زبان نوشتاری: انگلیسی
• ویرایش: 1  
• نویسنده: Janusz Pawliszyn
• تعداد صفحات: 477 صفحه 
• تعداد فصل ها: 13 فصل
• نحوه دریافت : دانلود فوری و آنی فایل بعد از پرداخت

 

فهرست مطالب و عناوین فصل های کتاب میکرو استخراج با فاز جامد

1. Solid-Phase Microextraction in Perspective

1.1. Sample Preparation as Part of the Analytical Process

1.2. Classification of Extraction Techniques

1.3. Perspective on Microextraction Techniques

1.4. Implementations of SPME

1.5. Miniaturisation and Integration

1.6. In Vivo Analysis

1.7. SPME Versus SPE

2. Theory of Solid-Phase Microextraction

2.1. Introduction

2.2. SPME Principle

2.3. Thermodynamics

2.4. Kinetics

2.5. Extraction with Derivatisation

2.6. Extraction of Sample Matrices Containing Solids

2.7. Solid Versus Liquid Sorbents

2.8. Passive TWA Sampling

2.9. In-Tube SPME

2.10. Experimental Verification

3. Development of SPME Devices and Coatings

3.1. Historical Perspective

3.2. Rational Design of SPME Devices

3.3. On-Site Samplers

3.4. Development of New SPME Coatings

3.5. Interfaces to Analytical Instrumentation

4. SPME Commercial Devices and Fibre Coatings

4.1. Introduction

4.2. Description of SPME Fibre Assemblies and Holders

4.3. Description of Fibre Cores, Coatings and the Coating Process

4.4. A Guide for the Selection of the Appropriate SPME Fibre

5. Automated SPME Systems

5.1. Automated Solid-Phase Microextraction–Gas Chromatography

5.2. Automated SPME–LC

5.3. Other Automated Configurations Involving SPME

6. Calibration

6.1. Introduction

6.2. Traditional Calibration Methods for the Quantification of SPME

6.3. Equilibrium Extraction

6.4. Exhaustive Extraction

6.5. Diffusion-Based Calibration

6.6. Calibration of SPME by Liquid Injection

6.7. Summary

7. Solid-Phase Microextraction Method Development

7.1. Introduction

7.2. SPME Method Development – General

7.3. SPME Method Development for GC Applications

7.4. SPME Method Development for HPLC Applications

7.5. Method Validation

7.6. Concluding Remarks

8. SPME and Environmental Analysis

8.1. Introduction

8.2. Fibre SPME

8.3. In-Tube SPME

8.4. TFME

8.5. Applications of SPME in Various Environmental Sample Matrices

8.6. Applications of SPME for Various Analytes in Environmental Samples

8.7. Concluding Remarks

9. Application of Solid-Phase Microextraction in Food and Fragrance Analysis

9.1. Introduction and Method Development Considerations

9.2. Reviews and Case Studies Involving SPME as an Extraction Procedure

9.3. Concluding Remarks

10. Drug Analysis by SPME

10.1. Introduction

10.2. Fundamentals of Extraction

10.3. Fibre Selection: Adsorption Versus Absorption

10.4. Considerations of Drug Properties

10.5. Calibration

10.6. Novel SPME Coatings for LC

10.7. Derivatisation

10.8. Instrumental Configurations

10.9. Applications

10.10. Conclusions

11. Ligand—Receptor Binding and Determination of Free Concentrations

11.1. Introduction

11.2. Analysis of Biological Samples

11.3. Determination of Free Concentrations and Binding Constants

11.4. Calibration of SPME for Bioanalytical Applications

11.5. Conclusions

12. In Vivo Sampling with Solid-Phase Microextraction

12.1. Introduction

12.2. In Vivo Method Development

12.3. In Vivo Applications

12.4. Conclusions

13. Solid-Phase Microextraction Protocols

13.1. Protocol for Automated High-Throughput SPME-LC using the Concept 96 Robotic Sample Preparation Station

13.2. Protocol for Automation of Ligand-Receptor Binding Studies Using Concept 96

13.3. In Vivo SPME Protocol for Direct Monitoring of Circulating Intravenous Blood Concentrations

13.4. Protocol for Setting up Automated SPME-GC Methods