دانلود کتاب روش های آنالیز حرارتی هاینس + حل المسائل

دانلود کتاب روش های آنالیز حرارتی هاینس + حل المسائل Thermal methods of analysis

کتاب روش های آنالیز حرارتی ، مبانی ، کاربردها و مسائل نوشته و تالیف هاینس ویرایش 1 اول Thermal methods of analysis : principles, applications and problems by P J Haines از کتاب های تخصصی و مرجع خوب و عالی در زمینه آنالیز و تجزیه حرارتی برای دانشجویان شیمی و مهندسی شیمی و همین طور اساتید این رشته می باشد.

حل المسائل شامل سوالات فصل 1 تا فصل 5 می باشد.

مشخصات کتاب

• عنوان کتاب: Thermal methods of analysis : principles, applications and problems
• فرمت فایل: PDF  با کیفیت بالا
• حجم فایل فشرده: 18.3 مگابایت
• ویرایش: 1
• زبان نوشتاری: انگلیسی
• نویسنده: P. J. Haines
• تعداد صفحات کتاب: 285 صفحه
• تعداد فصل ها: 6 فصل
• نحوه دریافت : دانلود فوری و آنی فایل بعد از پرداخت

فهرست مطالب و عناوین فصل های کتاب آنالیز حرارتی هاینس

1 Introduction to thermal methods
1.1 Introduction
1.2 Historical development
1.3 Definitions
1.3.1 Thermal analysis
1.3.2 Equilibrium
1.3.3 General apparatus
1.4 Computers and thermal methods
1.4.1 The Computer as an instructional tool
1.4.2 The Computer as a data gatherer
1.4.3 The Computer as a data processor
1.4.4 The Computer as a research tool
1.5 Factors affecting thermal analysis results
1.5.1 The sample
1.5.2 The crucible
1.5.3 The rate of heating
1.5.4 The atmosphere
1.5.5 The mass of the sample
1.6 Simultaneous and complementary techniques
1.7 Problems
References
General Bibliography
2 Thermogravimetry
2.1 Introduction
2.2 Historical
2.3 Definition of thermogravimetry
2.4 Apparatus
2.4.1 The balance
2.4.2 Furnace
2.4.3 Programmer
2.4.4 Samples
2.4.5 Temperature calibration
2.4.6 Atmosphere
2.5 Kinetics of reactions
2.5.1 Measurement of a and da/dt
2.6 Applications of thermogravimetry
2.6.1 Thermogravimetric curves
2.6.2 Analysis of mixtures
2.6.3 Oxidation studies
2.6.4 Reduction studies
2.7 Controlled rate thermogravimetry and Hi-Res™ TGA
2.7.1 Polymer blends
2.7.2 Fuel additives
2.7.3 Drugs
2.8 Problems
References
Bibliography
3 Differential thermal analysis and differential scanning calorimetry
3.1 Introduction
3.2 Historical
3.3 Definitions
3.3.1 Differential thermal analysis (DTA)
3.3.2 Differential scanning calorimetry (DSC)
3.4 Apparatus
3.4.1 The sensors
3.4.2 The furnace and Controller
3.4.3 The Computer and display
3.4.4 The reference material
3.5 Theory of DTA and DSC
3.6 Heat flux DSC
3.7 Power-compensated DSC
3.7.1 The effect of higher temperatures
3.7.2 Sample size
3.8 Calibration
3.9 Applications
3.9.1 Physical changes and measurements
3.9.2 Chemical reactions
3.9.3 Inorganic Compounds and complexes
3.9.4 Synthesis of Compounds at high temperatures
3.9.5 Pyrotechnics
3.9.6 Superconductors
3.9.7 Organic Compounds
3.10 Specialist DSC Systems
3.10.1 Pressure DSC (PDSC)
3.10.2 Photocalorimetric DSC
3.10.3 Modulated DSC (MDCSIM)
3.11 Problems
References
Bibliography
4 Thermomechanical, dynamic mechanical and associated methods
4.1 Introduction
4.2 Definitions
4.2.1 Thermomechanical analysis (TMA)
4.2.2 Dynamic mechanical analysis (DMA)
4.2.3 Mechanical moduli
4.3 Thermomechanical analysis
4.3.1 Apparatus
4.3.2 Applications
4.3.3 Chemical reactions 1394.4 Dynamic mechanical analysis
4.4.1 Apparatus
4.4.2 Applications
4.5 Dielectric thermal analysis
4.5.1 Definition of dielectric thermal analysis
4.5.2 Apparatus
4.5.3 Frequency ränge
4.5.4 Applications
4.6 Thermally stimulated current analysis and relaxation map analysis
4.6.1 Definition of thermally stimulated current analysis
4.6.2 Apparatus
4.6.3 Applications
4.7 Problems
References
Bibliography
5 Simultaneous techniques and product analysis
5.1 Introduction
5.2 Simultaneous thermal analysis
5.2.1 Simultaneous TG-DTA and TG-DSC
5.2.2 Applications
5.3 Evolved gas analysis
5.3.1 Instrumentation
5.3.2 Apparatus
5.4 Detection and identification of evolved gases
5.4.1 Physical methods
5.4.2 Chemical methods
5.4.3 Spectroscopic methods
5.4.4 Simultaneous thermal analysis-gas chromatography-mass
spectrometry
5.5 Infrared and simultaneous TA-infrared
5.5.1 Apparatus
5.5.2 Applications
5.5.3 Gas chromatography and pyrolysis GC-FTIR
5.6 Infrared product analysis
5.6.1 Application to polymer samples
5.6.2 Polymorphism
5.6.3 Metal complexes
5.7 Thermomicroscopy
5.7.1 Applications
5.7.2 Phase equilibria
5.7.3 Chemical reactions
5.7.4 Hydrated salts
5.8 X-ray methods
5.8.1 Applications
5.9 Electron microscopy and associated techniques
5.10 Conclusion
5.11 Less common thermal analysis techniques
5.12 Problems
References
Bibliography
6 Problem solving and applications of thermal methods
Introduction
List of examples
PROBLEMS/SOLUTIONS
Inorganic materials
Tin(II) formate decomposition
Mixtures of carbonates
Strontium nitrate decomposition
Calorimetry and phase transitions of potassium nitrate
Decomposition of barium Perchlorate
Solid-state reactions
Polymerie materials
Characterisation of a polymer
Polymer blend analysis
Kinetic studies of polymer eure
Polymer decomposition studies
Oxidative stability of polymers
Studies of epoxy-glass composite
Characterisation of a thin adhesive film
Fine chemicals and pharmaceuticals
Purity determination
Phase diagrams of organic chemicals
Liquid crystal studies
Stability and polymorphism of pharmaceuticals
Dynamic mechanical analysis of food produets
Other materials
Carbon oxidation
Proximate analysis of coals
Oil testing
Soil analysis
Catalyst studies
Survival of Antarctic micro-arthropods
Appendix: Solutions to problems in Chapters 1-5