NMR – From Spectra to Structures An Experimental Approach
- نویسنده: Mitchell, Terence N., Costisella, Burkhard
- حجم فایل فشرده: 4.78 مگابایت
- ویرایش: 2
- زبان نوشتاری: انگلیسی
- تعداد صفحات کتاب: 220 صفحه
- تعداد فصل ها: 8 فصل
- فرمت فایل: PDF با کیفیت بالا
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NMR – From Spectra to Structures An Experimental Approach
دانلود کتاب NMR از طیف تا ساختار NMR – From Spectra to Structures ویرایش 2
کتاب مرجع و تخصصی درباره طیف سنجی روزنانس مغناطیسی هسته NMR از طیف تا ساختار ،روش تجربی با عنوان NMR – From Spectra to Structures An Experimental Approach نوشته و تالیف Mitchell, Terence N., Costisella, Burkhard میچل ترنس و کاستیسلا بوکهارت ویرایش دوم ، بهترین منبع در زمینه آموزش طیف سنجی NMR می باشد. کسانی که می خواهند NMR را به خوبی یاد گیرند این کتاب را توصیه می کنیم.
مشخصات کتاب
فهرست مطالب و عناوین فصل های کتاب
Introduction
Part 1: NMR Experiments
1D Experiments
1H, D (2H): Natural Abundance, Sensitivity
Proton NMR Spectrum of the Model Compound 1
Field Dependence of the Spectrum of 1
FID Manipulation: FT, EM, SINE BELL (CH2 Signal of 1)
Te Proton Spectrum of 1 in D2O or H2O/D2O Mixtures
Integration: Relaxation, T1, 90°-Pulse, Ernst Angle
Te NOE: Trough-Space Interactions between Protons
NOE Difference Spectroscopy
Selective 1D NOE Experiment (1D-NOESY) and Selective 1D
TOCSY Experiment
Natural Abundance 13C Spectrum of Compound 1
Coupled Spectrum (Gated Decoupling)
Quantitative 13C Spectrum (Inverse Gated Decoupling)
Decoupled Spectrum: Proton Decoupling, Proton and Phosphorus
Decoupling
APT, DEPT, INEPT
Te INADEQUATE Experiment
Natural Abundance 31P Spectrum of Compound 6
Proton-Decoupled and Proton-Coupled Spectra
Coupled Spectrum (P–P Coupling)
2D Experiments
General Principles, Inverse Techniques, Gradients
2D NOE
P,H COSY: with Varying Mixing Times for the Coupling
C,H Direct Correlation
C,H Long Range Correlation
P,C Correlation
P,P Correlation
Quadrupolar Nucleus Experiments
General Principles: Quadrupole Moment, Relaxation, Linewidth
17O Spectrum of 7: Chemical Shif (Reference), Coupling with P
P–O Correlation
HPLC-NMR Coupling
General Principles, NMR as a Highly Sensitive Analytical Tool
(μg to ng Amounts)
Example: Separation of 4 and 5, Two Acetals of Formylphosphonic Ester
Chromatogram
On-Flow Diagram (Chemical Shif vs Time)
Stopped Flow Experiments
Other Spin-½ Nuclei
Solid State NMR
General Principles
Solid State 1H NMR
Solid State 13C NMR
Solid-State 31P NMR
Solid-State 29Si NMR
Solid State NMR
Appendix: Reference List
Part 2: Worked Example and Problems
Section 1
Solving the Structures of Organic Molecules
Elemental Analysis
Mass Spectrometry
Worked Example
H,H Correlation
C,H Correlation
Problems
Section 2
Introduction
Problems
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