دانلود هندبوک شیمی آلی سنتزی ویرایش 2 دوم Michael Pirrung

دانلود هندبوک شیمی آلی سنتزی ویرایش 2 دوم Michael Pirrung کتاب و هندبوک تخصصی شیمی آلی Handbook of Synthetic Organic Chemistry 2nd Edition تالیف مایکل پیرنگ Michael Pirrung جامع ترین هندبوک سنتزهای شیمی آلی که ویرایش جدید آن که توسط انتشارات elsevier در سال 2016 به چاپ رسیده است را با مشخصات زیر دانلود نمایید.

مشخصات کتاب

• عنوان انگلیسی:  Handbook of Synthetic Organic Chemistry 2nd Edition
• عنوان فارسی :  هندبوک شیمی آلی سنتزی
• فرمت فایل: PDF
• حجم فایل فشرده:  3.84 مگابایت
• ویرایش: 2 
• سال انتشار:  2016
• زبان نوشتاری: انگلیسی
• نویسنده(ها): Michael Pirrung
• تعداد صفحات:  290 صفحه
• تعداد فصل ها:  18 فصل
• نحوه دریافت : دریافت فوری و آنی لینک دانلود فایل بعد از پرداخت

فهرست مطالب و عناوین فصل های کتاب

Table of Contents
Foreword
Preface to the First Edition
Preface to the Second Edition
Acknowledgments
1. Safety
1.1. Training
1.2. Safety Data Sheets
1.3. Safety Pictograms
1.4. Personal Protective Equipment
1.5. General
2. Searching the Literature
2.1. Commercial Availability
2.2. Literature Preparations
2.3. Experimental Procedures
2.4. Other Electronic Resources for Synthetic Chemistry
3. Reagents
3.1. Short-Path Distillation
3.2. Ampules
3.3. Reagent Solutions
3.4. Titration
3.5. Reagent Storage
3.6. Subtle Reagent Variations
3.7. Dangerous Reagents
3.8. Reagent Properties
4. Gases
4.1. Lecture Bottles/Small Cylinders
4.2. Tanks or Cylinders
4.3. Gas Safety
5. Reactions on a Small Scale—1–25mmol
5.1. Reaction Flasks
5.2. Stirring
5.3. Glass Joints
5.4. Inert Atmosphere
5.5. Apparatus for Addition
5.6. Condensers
5.7. Other Equipment and Considerations
6. Temperature Control
6.1. Heating
6.2. Cooling
7. Solvents
7.1. Selection
7.2. Purity
7.3. Degassing
7.4. Ammonia
8. The Research Notebook
8.1. Paper Notebooks
8.2. Electronic Notebooks
9. Conducting the Reaction Itself
9.1. Reagents Supplied as Dispersions
9.2. Azeotropic Drying
9.3. Stoichiometry
9.4. Syringe and Inert Atmosphere Techniques
9.5. General Procedure for Transfer of Materials by Syringe
9.6. Addition
9.7. Special Techniques
9.8. Unattended Reactions
9.9. Quenching
9.10. Specialized Reagents
9.11. Checklist
9.12. Reaction Time Versus Purification Time
10. Following the Reaction
10.1. Thin Layer Chromatography
10.2. Gas Chromatography
10.3. High Performance Liquid Chromatography
10.4. Nuclear Magnetic Resonance Spectroscopy
11. Working Up Reactions
11.1. Solvent Extraction
11.2. Drying Organic Solutions
11.3. Specialized Workups
11.4. Destroying Reagents
12. Evaporation
13. Vacuum Systems
13.1. Vacuum Sources
13.2. Vacuum Manifolds
13.3. Vacuum Gauges
14. Purification of Products
14.1. Distillation
14.2. Silica Gel Chromatography
14.3. Flash Column Chromatography
14.4. Gradients
14.5. Special Adsorbents
14.6. Preparative Gas Chromatography
14.7. Precipitation
14.8. Trituration
14.9. Crystallization
14.10. Yields
15. Methods for Structure Elucidation
15.1. Nuclear Magnetic Resonance Spectroscopy
15.2. Infrared Spectroscopy
15.3. Ultraviolet Spectroscopy
15.4. Combustion Analysis
15.5. Mass Spectrometry
15.6. Optical Rotation
15.7. Chiral Chromatography
15.8. Crystal Growth for X-Ray
15.9. Novel Compound Characterization
16. Cleaning Up After the Reaction
16.1. Waste Disposal
16.2. Cleaning Equipment
17. Specific Example
17.1. The Experimental
17.2. The Org. Syn. Prep
17.3. Comparison
18. Strategies for Reaction Optimization
Appendix 1. Safety Protocols
Appendix 2. Synthetic Solvent Selection Chart
Appendix 3. Solvent Miscibility
Appendix 4. Freezing Points of Common Organic Solvents
Appendix 5. Toxicities of Common Organic Solvents
Appendix 6. Recipes for TLC Stains
Appendix 7. NMR Spectral Data of Common Contaminants of Organic and Organometallic Reaction Products
Appendix 8. Acidities of Organic Functional Groups
Appendix 9. Acidities of Organic Functional Groups in DMSO
Appendix 10. Stuck Joints
Index